21. November 2024.

Bruker Dimension Icon Scanning Probe Microscope (SPM)

  • AFM and STM modules in one device.

  • Supports contact and tapping mode (closed loop control keeps the force (deflection of the beam which holds the tip) constant, which limits the contact forces to < 200 pN, i.e. a value far lower than the tapping forces of other devices – PeakForce tapping).

  • Enables measurements of elasticity modulus, adhesion, lateral force (LFM), spectroscopy and force modulation, electrochemical analysis, electric field and magnetic forces, surface potential, piezoelectric force; enables also nanolitography, …

    Option to measure in liquid for biotechnical applications and measurements with heating/cooling of the samples, …

    Imaging of measured data on 5’120 x 5’120 pixels.

  • Samples fixed to the support via a vacuum chuck can be up to few millimetres in size, with bidirectional positioning repeatability of 3 μm on a scanning area of up to 90 x 90 μm.

  • Includes heat (creep < 200 pm/min) and vibration isolation (1” Si damping cushion + compressed air → < 30 pm RMS), microscope and CCD camera, control SW, …

  • PeakForce Tapping™ is an AC imaging technique, i.e., the cantilever is oscillated but well below resonance.

  • This results in a continuous series of force-distance curves.

  • In addition to direct force control by keeping the peak force constant, a multitude of material properties can be extracted and quantified from the force-distance curve at each pixel within an image, such as modulus, adhesion force, and deformation depth.

Examples of measurements – mechanical testing of orthodontic archwires (topographies of NiTi, Rh NiTi and N NiTi):

     

Examples of measurements – ball element and sliding surface of linear guideways:

 

Keysight G200 Nanoindenter

  • The device is thermally as well as dynamically (and acoustically) isolated.

  • Electromagnetic actuation (voice coil principle), i.e. load generation: max 0.5 N with a 50 nN resolution; additional built-in high-load system with 0.1 mN … 10 N load range. Loading system stiffness (guided by leaf springs): 5.106 N/m.

  • Capacitive displacement measurement: resolution < 0.01 nm for > 500 μm displacement range. Obtainable straightness in a 100 mm range is within 10 nm.

  • 4 samples in a 100 x 100 mm sample holder with a scanning resolution of 0.1 μm and 1 μm accuracy; automatically controlled (closed loop based on incremental encoders). Measurement of elasticity modulus and hardness according to ISO 14577.

  • Enables LFM with a ≤ 2 mN resolution and max lateral force

    ≥ 250 mN. Low-force measurements enable obtaining surface topology after indentation.

  • Berkovich, cube corner, conical, spherical and Vickers tips. System for sample visualization (10x and 40x zoom), microscope with CCD camera and data analysis SW.

Examples of measurements – mechanical testing of orthodontic archwires:

Shimadzu Autograph AGS-X micro-tensile machine

Measurement of mechanical properties (hardness, elasticity modulus, …) of metals, ceramics, polymers, rubber and composites up to 5 kN with 2 mN and 10 µm resolutions.

     

Examples of measurements – measurement of presliding friction of ultra-high precision positioning device:

Examples of measurements – mechanical testing of cured ham: